cholesterol p-phenylbenzoate

Base Information

• Chemical Name: cholesterol p-phenylbenzoate
• CAS No.: 35319-60-9
• Molecular Formula: C₄₀H₅₄O₂
• Molecular Weight: 566.868
• Mol file: 35319-60-9.mol

Synonyms:

Chemical Property of cholesterol p-phenylbenzoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of cholesterol p-phenylbenzoate

There total 4 articles about cholesterol p-phenylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cholesterol (57-88-5) + 4-biphenyl-carboxylic acid chloride (14002-51-8) → cholesterol p-phenylbenzoate (35319-60-9)

Guidance literature:

With pyridine; Ambient temperature;

DOI:10.1021/j100276a037

Reference yield:

biphenyl-4-acetaldehyde (92-91-1) → cholesterol p-phenylbenzoate (35319-60-9)

Guidance literature:

Multi-step reaction with 3 steps

1: hypobromite

2: phosphorous pentachloride

3: pyridine / benzene / 10 h / Ambient temperature

With pyridine; phosphorus pentachloride; hypobromite; In benzene;

DOI:10.1080/00268948208072592

Reference yield:

biphenyl-4-carboxylic acid (92-92-2) → cholesterol p-phenylbenzoate (35319-60-9)

Guidance literature:

Multi-step reaction with 2 steps

1: phosphorous pentachloride

2: pyridine / benzene / 10 h / Ambient temperature

With pyridine; phosphorus pentachloride; In benzene;

DOI:10.1080/00268948208072592

upstream raw materials:

pyridine

cholesterol

4-biphenyl-carboxylic acid chloride

cholesterol

Refernces

• 1、 Koden,Takenaka,Kusabayashi. "INFLUENCE OF THE ANGULAR LINKAGE ON THE MESOMORPHIC PROPERTIES OF CHOLESTERYL ARYLBENZOATES.". . p. 137 - 150. Retrieved 2007/10/02.