Technology Process of (S)-N1-((S)-1,5-diamino-1-imino-6,15-dioxo-2,7,12,16-tetraazahenicosan-21-yl)-2-(2-(2,4-dihydroxyphenyl)acetamido)-succinamide tris(2,2,2-trifluoroacetate)
There total 1 articles about (S)-N1-((S)-1,5-diamino-1-imino-6,15-dioxo-2,7,12,16-tetraazahenicosan-21-yl)-2-(2-(2,4-dihydroxyphenyl)acetamido)-succinamide tris(2,2,2-trifluoroacetate) which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
2-(trimethylsilyl)ethyl 5-aminopentylcarbamate;
With
2-(3,5-dimethoxy-4-formylphenoxy)ethyl polystyrene;
In
acetic acid; N,N-dimethyl-formamide;
for 0.0333333h;
2-(3,5-dimethoxy-4-formylphenoxy)ethyl polystyrene
With
sodium tris(acetoxy)borohydride;
In
acetic acid; N,N-dimethyl-formamide;
at 20 ℃;
2-(3,5-dimethoxy-4-formylphenoxy)ethyl polystyrene
(S)-2-(tert-butoxycarbonylamino)-5-(3-(2,2,4,6,7-pentamethyl-2,3-dihydrobenzofuran-5-ylsulfonyl)guanidino)pentanoic acid; N-[(o-nitrophenyl)sulfonyl]-β-alanine; 2-(2,4-bis(benzyloxy)phenyl)acetic acid; L-Asn(Trt); trifluoroacetic acid; 4-{N-[2-(Trimethylsilyl)ethoxycarbonyl]amino}butanol;
Further stages;
DOI:10.1021/jm301255m