Propylphosphonic acid dipropyl ester

Base Information

• Chemical Name: Propylphosphonic acid dipropyl ester
• CAS No.: 1789-95-3
• Molecular Formula: C9H21O3P
• Molecular Weight: 208.238
• Hs Code.: 2931900090
• Mol file: 1789-95-3.mol

Synonyms:propyl-phosphonic acid dipropyl ester;Propylphosphinsaeuredipropylester;Propyl-phosphonsaeure-dipropylester;Propan-phosphonsaeure-(1)-dipropylester;

Chemical Property of Propylphosphonic acid dipropyl ester

Chemical Property:

• Vapor Pressure: 0.0158mmHg at 25°C
• PSA: 45.34000
• LogP: 3.44270

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Propylphosphonic acid dipropyl ester

There total 8 articles about Propylphosphonic acid dipropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

propan-1-ol (71-23-8) + propylphosphonic acid (4672-38-2) → dipropyl propylphosphonate (1789-95-3)

Guidance literature:

With tetrachlorosilane; at 0 ℃;

DOI:10.1016/j.tetlet.2006.02.159

Reference yield: 90.0%

propan-1-ol (71-23-8) + propylphosphonic dichloride (4708-04-7) → dipropyl propylphosphonate (1789-95-3)

Guidance literature:

With aluminum oxide; at 20 ℃;

Reference yield:

propan-1-ol (71-23-8) + propylphosphonic acid (4672-38-2) → dipropyl propylphosphonate (1789-95-3) + monopropyl propylphosphonate (21921-97-1)

Guidance literature:

With 1-butyl-3-methylimidazolium Tetrafluoroborate; at 180 ℃; for 3.5h; Overall yield = 65 percent; Microwave irradiation; Green chemistry;

DOI:10.3390/molecules26175303

upstream raw materials:

triphenyl phosphite

propan-1-ol

1-iodo-propane

di-n-propyl phosphonate

Downstream raw materials:

propyl-phosphonic acid-(4-nitro-phenyl ester)-propyl ester

propanephosphonic acid dimethyl ester

Methyl propyl propylphosphonate

propyl tosylate

Refernces

• 1、 Gupta, Arvind K.,Kumar, Rajesh,Dubey, Devendra K.,Kaushik. "P-Toluenesulfonic acid-Celite as a reagent for synthesis of esters of alkylphosphonic acids under solvent-free conditions". . p. 328 - 331. Retrieved 2008/02/10.
• 2、 Acharya, Jyotiranjan,Shakya, Purushottam D.,Pardasani, Deepak,Palit, Meehir,Dubey, Devendra K.,Gupta, Arvind K.. "Surface-mediated solid phase reactions: A simple, efficient and base-free synthesis of phosphonates and phosphates on Al2O3". . p. 194 - 196. Retrieved 2007/10/03.