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Research on the synthesis of aromatic hydrazone in ionic liquids
Wang, Haibin,Sun, Li,Li, Xiaonian,Duan, Jiangli,Pei, Wen
experimental part, p. 3223 - 3227 (2011/09/30)
Aromatic hydrazones are important intermediates for pesticides cibenzoline and cefxime. The methodology of synthesis of aromatic hydrazone from aromatic ketone and hydrazine hydrate in ionic liquid, was described and various aromatic hydrazones were prepared by the reaction of aromatic ketone with hydrazine hydrate in ionic 1iquid at 100C with good yields. The ionic liquids could be recycled and reused after the reaction. The influences of the various ionic liquids on the reaction are discussed. The product structure was characterized by infrared, mass spectrometry, NMR spectra, and elemental analysis. Copyright