6395-23-9Relevant articles and documents
A protocol to generate phthaloyl peroxide in flow for the hydroxylation of arenes
Eliasen, Anders M.,Thedford, Randal P.,Claussen, Karin R.,Yuan, Changxia,Siegel, Dionicio
supporting information, p. 3628 - 3631 (2014/08/05)
A flow protocol for the generation of phthaloyl peroxide has been developed. This process directly yields phthaloyl peroxide in high purity (>95%) and can be used to bypass the need to isolate and recrystallize phthaloyl peroxide, improving upon earlier batch procedures. The flow protocol for the formation of phthaloyl peroxide can be combined with arene hydroxylation reactions and provides a method for the consumption of peroxide as it is generated to minimize the accumulation of large quantities of peroxide.
METHODS FOR THE PREPARATION OF SUBSTITUTED ACETOPHENONES
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Page/Page column 33, (2014/07/08)
The present application discloses novel methods for the preparation of pyrid-4-yl substituted acetophenones, in particular 2-{6-[2-(3,5-dichloro-pyridin-4-yl)-acetyl]-2,3-dimethoxy-phenoxy}-N-propyl-acetamide. The application also discloses novel stable c
Sequential removal of photolabile protecting groups for carbonyls with controlled wavelength
Wang, Pengfei,Wang, Yun,Hu, Huayou,Spencer, Cierra,Liang, Xing,Pan, Lurong
, p. 6152 - 6157 (2008/12/22)
(Chemical Equation Presented) A group of robust and easy-to-make photolabile protecting groups (PPGs) for carbonyl compounds has been developed. Sequential removal of different PPGs is achieved via control of irradiation wavelength.