97828-25-6Relevant articles and documents
Facile synthesis of norwogonin, isoscutellarein, and herbacetin
Yuan, Hu,Ye, Ji,Chen, Hao,Zhao, Zeng,Luo, Xukai,Zhang, Weidong,Sun, Qingyan
, p. 3389 - 3391 (2016)
An expeditious synthesis of norwogonin, isoscutellarein, and herbacetin, has been accomplished by a strategy featuring a borylation of sterically hindered aryl iodide and a one-pot oxidation to generate the C-3 and C-8 OH groups. The total synthesis gives excellent yields and conventional flash column chromatography is not needed for purification.
Preparation method of flavonoids
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Paragraph 0213-0217; 0219-0220, (2017/11/16)
The invention discloses a preparation method of flavonoids. The method comprises the following step: in a solvent, in the presence of iodine and a silver salt or in the presence of iodine and a copper salt, performing an iodination reaction on a compound 1 to obtain a compound 2. Raw materials used in the method are easy to acquire, and the method has high yields and simple post processes, and does not need column chromatography.