9-Bromo-10-phenylanthracene (23674-20-6) production

Trusyn Chem-Tech Co., Ltd. guanrantees 9-Bromo-10-phenylanthracene production with sufficient capital resource, excellent technicians, qualified labor force, sufficient resources, advanced equipments and environmental technology in their factory. They are based on technology and create values for the society; looks into the future and renovate technologies. While creating values for ourselves, they create career for employees, create benefit for customers and values for the society.

9-Bromo-10-phenylanthracene (23674-20-6) Synthesis

A mixture of 9,10-dibromoanthracene, phenylboronic acid and tetrakis(triphenylphosphine) palladium was added to an air-free two-phase mixture of THF and aqueous 2 M K2CO3. The resulting mixture was vigorously stirred under nitrogen atmosphere at 80 ℃ for 8 h. The organic layer was separated and the aqueous phase was extracted with dichloromethane , the combined organic layer was washed with brine and dried over anhydrous MgSO4. The solvent was evaporated under reduced pressure to give an light-yellow solid, which was further purified with column chromatography using petroleum ether/dichloromethane as eluant to afford the target product.