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5. An oven-dried Schlenk tube was charged with the aryl halide (2
mmol) and amine (2.5 mmol), Fe@OA-Pd (0.05 g, 0.04 mmol, 1.5
mol%), base (3 mmol), solvent (5 mL) and additive. The resulting
mixture was stirred for the appropriate time and temperature. After
reaction completion the reaction mixture was then cooled to room
temperature and the catalyst separated using a magnet, taken up in
Et
2
O (4 mL), and washed with brine (5 mL). The resulting solution
, filtered and concentrated. The
was dried over anhydrous MgSO
4
crude product was purified by flash chromatography on silica gel.
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