Journal of Fluorine Chemistry p. 257 - 264 (1980)
Update date:2022-08-25
Topics:
Katsuhara,Yutaka
Desmarteau, Darryl D.
The synthesis of the first trifluoromethanesulfonate esters of the type CF3SO3(CH2)nO3SCF3(n=1,2,3) are reported.The new compounds are prepared from Cl(CH2)nCl by substitutive electrophilic dehalogenation reactions with CF3SO2OX (x=Cl,Br).The extension of this reaction to HCCl3 results in HC(O3SCF3)3 but the compound is unstable at 22 deg.
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