ethyl ester of 7-hydroxyheptanoic acid

Base Information

• Chemical Name: ethyl ester of 7-hydroxyheptanoic acid
• CAS No.: 6149-48-0
• Molecular Formula: C9H18 O3
• Molecular Weight: 174.24
• Mol file: 6149-48-0.mol

Synonyms:7-Hydroxyheptanoicacid ethyl ester; Ethyl 7-hydroxyheptanoate

Chemical Property of ethyl ester of 7-hydroxyheptanoic acid

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 130.17000
• Density: 1.31g/cm³
• LogP: 3.39310

Purity/Quality:

99.00% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ethyl ester of 7-hydroxyheptanoic acid

There total 18 articles about ethyl ester of 7-hydroxyheptanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

ethanol (64-17-5) + 7-hydroxyheptanal (22054-13-3) → ethyl 7-hydroxyheptanoate (6149-48-0)

Guidance literature:

With Pt/γ-Al2O3; In toluene; at 100 ℃; Temperature; Reagent/catalyst; Solvent;

Reference yield: 85.0%

ethanol (64-17-5) + cycloheptanone (502-42-1) → ethyl 7-hydroxyheptanoate (6149-48-0)

Guidance literature:

With dipotassium peroxodisulfate; sulfuric acid; In water; for 5h; Ambient temperature;

DOI:10.1080/00397919108019797

Reference yield: 83.0%

7-hydroxyheptanoic acid (3710-42-7) + ethanol (64-17-5) → ethyl 7-hydroxyheptanoate (6149-48-0)

Guidance literature:

With sulfuric acid; Heating;

DOI:10.1007/BF00960290

upstream raw materials:

cycloheptanone

7-ethoxy-7-oxoheptanoic acid

trifluoroacetic acid

ethanol

Downstream raw materials:

7-hydroxy-heptanoic acid hydrazide

Octadec-17-ensaeure

ethyl 6-heptenoate

6,8-dichlorooctanoic acid ethyl ester

Refernces

• 1、 -. "Method for preparing 6,8-dichloroethyl caprylate". Paragraph 0045; 0046-0047; 0052-0053; 0058-0059. . Retrieved 2021/03/13.
• 2、 Ruan, Qiao,Zhou, Le,Breit, Bernhard. "New phosphorus self-assembling ligands for the tandem hydroformylation- Wittig olefination reaction of homoallylic alcohols - A key step for stereoselective pyran synthesis". . p. 87 - 90. Retrieved 2014/07/07.