Pt(C₈H₄N₂O(C₆H₅)(CH₂CO₂))2

Base Information

• Chemical Name: Pt(C₈H₄N₂O(C₆H₅)(CH₂CO₂))2
• CAS No.: 122896-60-0
• Molecular Formula: C₃₂H₂₂N₄O₆Pt
• Molecular Weight: 753.63
• Mol file: 122896-60-0.mol

Synonyms:

Chemical Property of Pt(C₈H₄N₂O(C₆H₅)(CH₂CO₂))2

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Pt(C₈H₄N₂O(C₆H₅)(CH₂CO₂))2

There total 2 articles about Pt(C₈H₄N₂O(C₆H₅)(CH₂CO₂))2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

platinum(II) chloride (10025-65-7) + (2-Phenyl-3,4-dihydro-4-oxoquinazolin-3-yl)acetic acid (65925-10-2) → {platinum(II)(2-phenylquinazoline-(3H)-4-one-3-CH2COO)2} (122896-60-0)

Guidance literature:

In hydrogenchloride; methanol; dropwise addn. of the quinazoline compd. in MeOH to PtCl2 in aqueous HCl under stirring and refluxing for about 30-60 min.; cooling, filtn., washing with hot water and MeOH and drying (vac. over fused CaCl2); elem. anal.;

Reference yield:

platinum(II) chloride (10025-65-7) + (2-Phenyl-3,4-dihydro-4-oxoquinazolin-3-yl)acetic acid (65925-10-2) → Pt(C8H4N2O(C6H5)(CH2CO2))2 (122896-60-0)

Guidance literature:

In hydrogenchloride; dropwise addn. of ligand soln. in MeOH or acetone to a soln. of PtCl2 in aq. HCl with constant stirring; cooling, filtration of solid, washing (H2O, MeOH/acetone) until free of ligand, drying in vac. over fused CaCl2, elem. anal.;

upstream raw materials:

platinum(II) chloride

(2-Phenyl-3,4-dihydro-4-oxoquinazolin-3-yl)acetic acid

Refernces