Carbonochloridic acid, 1,2-ethanediylbis(oxy-2,1-ethanediyl) ester

Base Information

• Chemical Name: Carbonochloridic acid, 1,2-ethanediylbis(oxy-2,1-ethanediyl) ester
• CAS No.: 17134-17-7
• Molecular Formula: C8H12 Cl2 O6
• Molecular Weight: 275.086
• Hs Code.: 29159000
• European Community (EC) Number: 628-141-9
• DSSTox Substance ID: DTXSID5066164
• Nikkaji Number: J421.984H
• Wikidata: Q81992745
• Mol file: 17134-17-7.mol

Synonyms:17134-17-7;Triethylene glycol bis(chloroformate);Tri(ethylene glycol) bis(chloroformate);Carbonochloridic acid, 1,2-ethanediylbis(oxy-2,1-ethanediyl) ester;2-[2-(2-carbonochloridoyloxyethoxy)ethoxy]ethyl carbonochloridate;Triethylene glycol bischloroformate;TRIETHYLENEGLYCOLBIS(CHLOROFORMATE);SCHEMBL33420;Carbonochloridic acid, diester with triethylene glycol;DTXSID5066164;GEO-02364;MFCD00011536;AKOS005258238;MS-20866;FT-0745373;Tri(ethylene glycol) bis(chloroformate), 97%;2,2'-(ethane-1,2-diylbis(oxy))bis(ethane-2,1-diyl) dicarbonochloridate;Carbonochloridic acid, C,C'-(1,2-ethanediylbis(oxy-2,1-ethanediyl)) ester

Chemical Property of Carbonochloridic acid, 1,2-ethanediylbis(oxy-2,1-ethanediyl) ester

Chemical Property:

• Appearance/Colour: clear colourless to brown liquid
• Vapor Pressure: 0.09 psi ( 20 °C)
• Refractive Index: n20/D 1.457(lit.)
• Boiling Point: 334.3 °C at 760 mmHg
• Flash Point: 134.8 °C
• PSA: 52.49000
• Density: 1.354 g/cm³
• LogP: 5.33000
• Storage Temp.: 0-6°C
• XLogP3: 1.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 11
• Exact Mass: 274.0010935
• Heavy Atom Count: 16
• Complexity: 189

Purity/Quality:

≥95% ^*data from raw suppliers

Tri(ethylene glycol) bis(chloroformate) 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s): T
• Hazard Codes: T
• Statements: 23/24/25-34
• Safety Statements: 26-27-36/37/39-45

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: C(COCCOC(=O)Cl)OCCOC(=O)Cl

Technology Process of Carbonochloridic acid, 1,2-ethanediylbis(oxy-2,1-ethanediyl) ester

There total 2 articles about Carbonochloridic acid, 1,2-ethanediylbis(oxy-2,1-ethanediyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phosgene (75-44-5) + 2,2'-[1,2-ethanediylbis(oxy)]bisethanol (112-27-6) → triethylene glycol bis(chloroformate) (17134-17-7)

Guidance literature:

cooling;

DOI:10.1081/SCC-100000525

Reference yield:

→ triethylene glycol bis(chloroformate) (17134-17-7)

Guidance literature:

Reference yield: 97.0%

triethylene glycol bis(chloroformate) (17134-17-7) → 1,2-bis(2-chloroethoxy)ethane (112-26-5,27252-69-3)

Guidance literature:

With hexabutylguanidinium chloride; at 120 ℃; for 4h;

DOI:10.1081/SCC-100000525

upstream raw materials:

phosgene

2,2'-[1,2-ethanediylbis(oxy)]bisethanol

Downstream raw materials:

C₂₄H₂₄I₆N₄O₁₀

bis(phenylmethyl) 8,13,24,29-tetraoxo-12,25-bis<2-<<1-oxo-6-<<(phenylmethoxy)carbonyl>amino>hexyl>amino>ethyl>-14,17,20,23-tetraoxa-2,9,12,25,28,35-hexaazahexatriacontanedioate

Refernces

• 1、 -. "Synthetic multimerizing agents". . . Retrieved 2008/06/13.