Tris(2,4-dibromophenyl)amine

Base Information

• Chemical Name: Tris(2,4-dibromophenyl)amine
• CAS No.: 5489-72-5
• Molecular Formula: C18H9Br6N
• Molecular Weight: 718.7
• DSSTox Substance ID: DTXSID00466768
• Nikkaji Number: J1.549.584G
• Wikidata: Q82293392
• Mol file: 5489-72-5.mol

Synonyms:tris(2,4-dibromophenyl)amine;5489-72-5;Benzenamine, 2,4-dibromo-N,N-bis(2,4-dibromophenyl)-;2,4-dibromo-N,N-bis(2,4-dibromophenyl)aniline;SCHEMBL1874361;DTXSID00466768;FT-0741279;E85166

Chemical Property of Tris(2,4-dibromophenyl)amine

Chemical Property:

• XLogP3: 9.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 3
• Exact Mass: 718.57738
• Heavy Atom Count: 25
• Complexity: 376

Purity/Quality:

99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=C(C=C1Br)Br)N(C2=C(C=C(C=C2)Br)Br)C3=C(C=C(C=C3)Br)Br

Technology Process of Tris(2,4-dibromophenyl)amine

There total 6 articles about Tris(2,4-dibromophenyl)amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

N,N-diphenylaminobenzene (603-34-9) → Tris(2,4-dibromophenyl)amine (5489-72-5)

Guidance literature:

With bromine; In chloroform; Ambient temperature;

DOI:10.1021/ja00126a007

Reference yield: 80.0%

tri(p-bromophenyl)amine (4316-58-9) → Tris(2,4-dibromophenyl)amine (5489-72-5)

Guidance literature:

With bromine; In chloroform; Ambient temperature;

Reference yield: 66.0%

benzyl decanoate (42175-41-7) → 1-decanoic acid (334-48-5) + Tris(2,4-dibromophenyl)amine (5489-72-5) + benzaldehyde (100-52-7)

Guidance literature:

With 2b⁽¹⁺⁾(.); sodium hydrogencarbonate; In water; acetonitrile; Yield given; indirect electrolysis;

upstream raw materials:

benzyl decanoate

tri(p-bromophenyl)amine

N,N-diphenylaminobenzene

Downstream raw materials:

Tris(2,4,6-tribromphenyl)amin

Refernces

• 1、 Yueh, Wang,Bauld, Nathan L.. "Mechanistic criteria for cation radical reactions: Aminium salt-catalyzed cyclopropanation". . p. 5671 - 5676. Retrieved 2007/10/02.
• 2、 Schmidt, Werner,Steckhan, Eberhard. "Organic Electron Transfer Agents, I. Electrochemical and Spectroscopical Study of Bromo-substituted Triarylamine Redox Systems". . p. 577 - 585. Retrieved 2007/10/02.