N1-(2-Aminoethyl)-N2-(3-(trimethoxysilyl)propyl)ethane-1,2-diamine

Base Information

• Chemical Name: N1-(2-Aminoethyl)-N2-(3-(trimethoxysilyl)propyl)ethane-1,2-diamine
• CAS No.: 35141-30-1
• Deprecated CAS: 153405-87-9,71663-05-3,2079786-40-4,2101977-05-1
• Molecular Formula: C10H27N3O3Si
• Molecular Weight: 265.428
• Hs Code.: 29319090
• European Community (EC) Number: 252-390-9
• UNII: 3W3E2D4706
• DSSTox Substance ID: DTXSID2044422
• Nikkaji Number: J289.914K
• Wikidata: Q27258112
• ChEMBL ID: CHEMBL3561898
• Mol file: 35141-30-1.mol

Synonyms:3-(2-(2-aminoethyl)-ethylamino)-propyl-trimethoxysilane;3-(2-(2-aminoethyl)ethylamino)propyltrimethoxysilane;AEEA cpd

Chemical Property of N1-(2-Aminoethyl)-N2-(3-(trimethoxysilyl)propyl)ethane-1,2-diamine

Chemical Property:

• Appearance/Colour: Clear, light to dark yellow liquid
• Vapor Pressure: 1 mm Hg ( 20 °C)
• Refractive Index: n20/D 1.459(lit.)
• Boiling Point: 321.938 °C at 760 mmHg
• PKA: 10.17±0.19(Predicted)
• Flash Point: 148.503 °C
• PSA: 77.77000
• Density: 0.984 g/cm³
• LogP: 0.87460
• Water Solubility.: 1000g/L at 20℃
• Hydrogen Bond Donor Count: 3
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 12
• Exact Mass: 265.18216827
• Heavy Atom Count: 17
• Complexity: 163

Purity/Quality:

99% ^*data from raw suppliers

3-[(Trimethoxysilyl)propyl]diethylenetriamine ^*data from reagent suppliers

Safty Information:

• Pictogram(s): C
• Hazard Codes: C
• Statements: 21-34-43-14
• Safety Statements: 26-36/37/39-45-8-30-24/25

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Chemical Classes: Metals -> Metalloid Compounds (Silicon)
• Canonical SMILES: CO[Si](CCCNCCNCCN)(OC)OC
• Uses: N1-(3-Trimethoxysilylpropyl)diethylenetriamine (TRI-silane) can be used as a grafting agent to incorporate amine functional group onto the surface of various ordered mesoporous silica. It can be also used in CO2 capture applications.

Technology Process of N1-(2-Aminoethyl)-N2-(3-(trimethoxysilyl)propyl)ethane-1,2-diamine

There total 2 articles about N1-(2-Aminoethyl)-N2-(3-(trimethoxysilyl)propyl)ethane-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-azapentane-1,5-diamine (111-40-0,98824-35-2) + 3-Chloropropyltrimethoxysilan (2530-87-2) → (3-trimethoxysilylpropyl)diethylenetriamine (35141-30-1)

Guidance literature:

3-azapentane-1,5-diamine; 3-Chloropropyltrimethoxysilan; at 125 - 130 ℃; for 8h;

With sodium methylate; In methanol; at 25 ℃; for 3h; Concentration; Reagent/catalyst; Solvent;

Reference yield:

→ (3-trimethoxysilylpropyl)diethylenetriamine (35141-30-1)

Guidance literature:

Reference yield: 96.0%

toluene diisocyanate trimer (98474-79-4) + (3-trimethoxysilylpropyl)diethylenetriamine (35141-30-1) → C37H45N9O9Si

Guidance literature:

With dibutyltin dilaurate; In tetrahydrofuran; at 20 ℃; for 5h; Dry environment;

upstream raw materials:

3-azapentane-1,5-diamine

3-Chloropropyltrimethoxysilan

Downstream raw materials:

C₁₇H₃₁N₃O₄Si

Refernces

• 1、 -. "Process for manufacturing polysiloxane microcapsules that are functionalized and are not very porous". Page/Page column 3. . Retrieved 2016/09/26.
• 2、 -. "Azido-silane compositions". . . Retrieved 2008/06/13.