Technology Process of [(2-Methylpropyl)selanyl]benzene
There total 5 articles about [(2-Methylpropyl)selanyl]benzene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
diphenyl diselenide;
In
benzene;
byproducts: Hg(SePh)2; Irradiation (UV/VIS); nitrogen atmosphere; mercurial and PhSeSePh (1.2 equiv) in deoxygenated solvent irradiated (275-W sunlamp, 35-40 °C, 5h);; filtration; solvent removed (vacuum); yield detd. by GLC after aq. Na2S2O3/CH2Cl2 extn.; i-BuSePh analysed by (1)H NMR, GLC and GCMS;;
DOI:10.1021/ja00219a030
- Guidance literature:
-
With
[{Ti(salophen)H2O}2O][OSO2C4F9]2; zinc;
In
tetrahydrofuran;
at 20 ℃;
for 2h;
Inert atmosphere;
DOI:10.1016/j.tet.2019.130750