1-DIPHENYLMETHYL-4-NITROSOPIPERAZINE

Base Information

• Chemical Name: 1-DIPHENYLMETHYL-4-NITROSOPIPERAZINE
• CAS No.: 1698-25-5
• Molecular Formula: C17H19 N3 O
• Molecular Weight: 281.35
• Hs Code.: 2933599090
• Mol file: 1698-25-5.mol

Synonyms:1-Diphenylmethyl-4-nitrosopiperazine;SC 11808

Chemical Property of 1-DIPHENYLMETHYL-4-NITROSOPIPERAZINE

Chemical Property:

• Vapor Pressure: 1.29E-07mmHg at 25°C
• Boiling Point: 430.5°Cat760mmHg
• Flash Point: 214.1°C
• PSA: 35.91000
• Density: 1.15g/cm³
• LogP: 2.95080

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-DIPHENYLMETHYL-4-NITROSOPIPERAZINE

There total 2 articles about 1-DIPHENYLMETHYL-4-NITROSOPIPERAZINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

diphenylmethylpiperazine (841-77-0) → 1-benzhydryl-4-nitrosopiperazine (1698-25-5)

Guidance literature:

With tert.-butylnitrite; In neat (no solvent); at 45 ℃; for 8h; chemoselective reaction; Green chemistry;

DOI:10.1039/c5gc02880a

Reference yield:

→ 1-benzhydryl-4-nitrosopiperazine (1698-25-5)

Guidance literature:

entspr. Piperazin, NaNO2, HCl;

DOI:10.1002/jps.2600670707

upstream raw materials:

diphenylmethylpiperazine

Refernces

• 1、 Yung,Gilroy,Mahony. "Synthesis and quantitative structure-activity relationships of antibacterial 1-(substituted benzhydryl)-4-(5-nitro-2- furfurylideneamino)piperazines". . p. 900 - 905. Retrieved 2007/10/04.