1,1':3',1''-Tercyclohexane

Base Information

• Chemical Name: 1,1':3',1''-Tercyclohexane
• CAS No.: 1706-50-9
• Molecular Formula: C18H32
• Molecular Weight: 248.452
• Hs Code.: 2902199090
• Mol file: 1706-50-9.mol

Synonyms:1,3-Dicyclohexylcyclohexane;1,3-Tercyclohexyl; NSC 114849; m-Tercyclohexane; m-Tercyclohexyl

Chemical Property of 1,1':3',1''-Tercyclohexane

Chemical Property:

• Melting Point: 62.5-63.5 °C
• Boiling Point: 341.6°Cat760mmHg
• Flash Point: 147.7°C
• PSA: 0.00000
• Density: 0.931g/cm³
• LogP: 5.95340

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,1':3',1''-Tercyclohexane

There total 11 articles about 1,1':3',1''-Tercyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,3-diphenylbenzene (92-06-8) → perhydro-meta-terphenyl (1706-50-9)

Guidance literature:

With nickel; at 200 ℃; under 73550.8 Torr; Hydrogenation;

DOI:10.1021/ja01271a003

Reference yield:

1-Phenyl-3-cyclohexyl-cyclohexan (20273-26-1,33460-02-5) → perhydro-meta-terphenyl (1706-50-9)

Guidance literature:

With hydrogen; nickel; at 180 ℃; under 76000 Torr;

Reference yield:

1,3-diphenylbenzene (92-06-8) → perhydro-meta-terphenyl (1706-50-9)

Guidance literature:

at 200 ℃; under 73550.8 Torr; Hydrogenation;

DOI:10.1021/ja01271a003

upstream raw materials:

1,3-diphenylbenzene

3,5-diphenylcyclohex-2-en-1-one

1-Phenyl-3-cyclohexyl-cyclohexan

methyl cyclohexane

Downstream raw materials:

1,3-diphenylbenzene

1,3-dicyclohexylbenzene

1,3-diphenyl-cyclohexane

3-cyclohexyl-1,1'-biphenyl

Refernces

• 1、 Kalenchuk,Bogorodskii,Bogdan. "Kinetic and thermodynamic parameters of hydrogen release during the heterogeneous catalytic dehydrogenation of cis- and trans-isomers of perhydro-m-terphenyl". . p. 1921 - 1924. Retrieved 2016.