GLYOXIME

Base Information Edit

Chemical Name:GLYOXIME
CAS No.:557-30-2
Molecular Formula:C2H4 N2 O2
Molecular Weight:88.066
Hs Code.:29280000
Mol file:557-30-2.mol

Synonyms:Ethanedial,dioxime (9CI); Glyoxal, dioxime (8CI); Glyoxime (6CI,7CI); Ethanedione dioxime;NSC 18263; Pik-off

Suppliers and Price of GLYOXIME

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
Glyoxime
2.5g
$ 110.00

American Custom Chemicals Corporation
GLYOXIME 95.00%
25G
$ 1158.18

Alfa Aesar
Glyoxime, 98+%, moistened with ca 20% water
50g
$ 223.00

Alfa Aesar
Glyoxime, 98+%, moistened with ca 20% water
10g
$ 57.20

Total 24 raw suppliers

Chemical Property of GLYOXIME Edit

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Melting Point:178-180 °C
Refractive Index:1.4300 (estimate)
Boiling Point:169.3°Cat760mmHg
PKA:9.90±0.10(Predicted)
Flash Point:56.2°C
PSA：65.18000
Density:1.29g/cm³
LogP:-0.09360
Solubility.:DMSO, Water

Purity/Quality:

99%, ^*data from raw suppliers

Glyoxime ^*data from reagent suppliers

Safty Information:

Pictogram(s): R1:Explosive when dry.; R11:Highly flammable.; R21:Harmful in contact with skin.; R25:Toxic if swallowed.;
Hazard Codes:R1:Explosive when dry.; R11:Highly flammable.; R21:Harmful in contact with skin.; R25:Toxic if swallowed.;
Statements: 1-11-21-25
Safety Statements: 16-35-36/37/39-45

MSDS Files:: SDS file from LookChem

Useful:

Uses Ethanedione Dioxime is an nitroso vinyl amine used in the synthesis of various nitriles.

Technology Process of GLYOXIME

There total 31 articles about GLYOXIME which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 131543-46-9,107-22-2
Glyoxal

: 557-30-2
glyoxime

Guidance literature:: With hydroxylamine hydrochloride; sodium hydroxide; In water; at 0 ℃; for 0.666667h; Inert atmosphere; Schlenk technique;
DOI:10.1021/acs.joc.0c00326

Reference yield:

: 107-15-3,85404-18-8
ethylenediamine

: 557-30-2
glyoxime

: 131543-46-9,107-22-2
Glyoxal

Guidance literature:: With [(-Ti(H₂O)(OH)-O-Ti(H₂O)(OH)-O-)*(O*-O^-)]n; dihydrogen peroxide; In methanol; at 25 ℃; for 0.75h;
DOI:10.1002/1521-3773(20010119)40:2<405::AID-ANIE405>3.0.CO;2-6