1-Propanesulfonyl chloride

Base Information

• Chemical Name: 1-Propanesulfonyl chloride
• CAS No.: 10147-36-1
• Molecular Formula: C3H7ClO2S
• Molecular Weight: 142.606
• Hs Code.: HYSICAL AND CHEMICAL PROPERTIES PHYSICAL STATE clear liquid
• European Community (EC) Number: 233-414-7
• UNII: MHH8GN4LBV
• DSSTox Substance ID: DTXSID4064973
• Nikkaji Number: J192.746I
• Wikidata: Q72502260
• Mol file: 10147-36-1.mol

Synonyms:1-Propanesulfonyl chloride;10147-36-1;Propane-1-sulfonyl chloride;Propanesulfonyl chloride;Propanesulphonyl chloride;1-Propane Sulfonyl Chloride;C3H7ClO2S;n-propanesulfonyl chloride;propylsulfonyl chloride;MHH8GN4LBV;MFCD00007462;propane-1-sulfonylchloride;n-propanesulphonyl chloride;1-propanesulphonyl chloride;EINECS 233-414-7;1-propanesulfonylchloride;n-PrSO2Cl;propanesulfonylchloride;Propanesufonyl chloride;propane-sulfonylchloride;1-propylsulfonylchloride;UNII-MHH8GN4LBV;n-propylsulfonyl chloride;propane-sulfonyl chloride;Propane sulfonyl chloride;1-propansulfonyl chloride;n-C3H7SO2Cl;n-propylsulphonyl chloride;propane-1-sulfonyl choride;n-propane sulfonyl chloride;propane-1-sulphonylchloride;1 -propanesulfonyl chloride;propanesulfonic acid chloride;propylsulphonic acid chloride;1-propane sulphonyl chloride;propan-1-ylsulfonyl chloride;SCHEMBL177337;1-propanesulfonic acid chloride;DTXSID4064973;1-Propanesulfonyl chloride, 97%;PROPAN-1-SULFONYL CHLORIDE;PROPAN-1-SULPHONYL CHLORIDE;AMY39421;BBL027643;STK503665;AKOS000119915;AS-14032;FT-0658140;P0693;EN300-20712;N10374;A800393;J-000404;F2190-0561

Chemical Property of 1-Propanesulfonyl chloride

Chemical Property:

• Appearance/Colour: clear liquid
• Vapor Pressure: 0.675mmHg at 25°C
• Melting Point: -46oC
• Refractive Index: n20/D 1.453(lit.)
• Boiling Point: 192.6 °C at 760 mmHg
• Flash Point: 64.9 °C
• PSA: 42.52000
• Density: 1.29 g/cm³
• LogP: 2.04580
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C
• Sensitive.: Moisture Sensitive
• Water Solubility.: Decomposes in hot water.
• XLogP3: 1.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 141.9855283
• Heavy Atom Count: 7
• Complexity: 120

Purity/Quality:

98% ^*data from raw suppliers

1-Propanesulfonyl Chloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s): C
• Hazard Codes: C
• Statements: 14-34-36-R36-R34-R14
• Safety Statements: 26-36/37/39-45-S45-S36/37/39-S26

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: CCCS(=O)(=O)Cl
• Uses: 1-Propanesulfonyl chloride was used in synthesis of 1-alkyl-3-methylimidazolium alkanesulfonate ionic liquids.

Technology Process of 1-Propanesulfonyl chloride

There total 14 articles about 1-Propanesulfonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

Dipropyl disulfide (629-19-6) → n-propanesulfonyl chloride (10147-36-1)

Guidance literature:

With chloro-trimethyl-silane; potassium nitrate; In dichloromethane; at 50 ℃; for 4h;

DOI:10.1021/jo070907g

Reference yield:

propanesulfonic acid (5284-66-2) → n-propanesulfonyl chloride (10147-36-1)

Guidance literature:

With phosphorus pentachloride;

DOI:10.1007/BF00898783

Reference yield:

→ n-propanesulfonyl chloride (10147-36-1)

Guidance literature:

With water; chlorine; at 10 - 15 ℃;

upstream raw materials:

propyl thiocyanate

propane

propanesulfonic acid

1-thiopropane

Downstream raw materials:

trans-1,4-bis-(propane-1-sulfonyloxy)-cyclohexane

propane-1-sulfonamide

1-perfluoropropanesulfonyl fluoride

Dipropyl disulfide

Refernces

• 1、 Pantlitschko,Salvenmoser. "-". . p. 285. Retrieved 1958.
• 2、 Benfodda, Zohra,Guillen, Franck,Arnion, Helene,Dahmani, Abdelkader,Blancou, Hubert. "A new synthesis of alkane and polyfluoroalkanesulfonyl chlorides". . p. 355 - 361. Retrieved 2009.
• 3、 Prakash, G. K. Surya,Mathew, Thomas,Panja, Chiradeep,Olah, George A.. "Chlorotrimethylsilane-nitrate salts as oxidants: Direct oxidative conversion of thiols and disulfides to sulfonyl chlorides". . p. 5847 - 5850. Retrieved 2008/02/09.