Technology Process of 5-(4-bromophenyl)-2-methylpentan-2-ol
There total 4 articles about 5-(4-bromophenyl)-2-methylpentan-2-ol which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
methylmagnesium bromide; 4-(4-bromophenyl)butanoic acid methyl ester;
In
diethyl ether;
for 15h;
With
water; ammonium chloride;
In
diethyl ether;
DOI:10.1016/j.bmc.2009.05.035
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 100 percent / p-toulenesulphonic acid / benzene / Heating
2: MeMgI / diethyl ether / 24 h / Ambient temperature
With
methyl magnesium iodide; toluene-4-sulfonic acid;
In
diethyl ether; benzene;
DOI:10.1016/S0040-4020(01)96390-2
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 44 percent / AlCl3 / 5 h / 90 °C
2: 70 percent / Zn-Hg, cc. HCl / 185 - 190 °C / 1.5 Torr
3: 100 percent / p-toulenesulphonic acid / benzene / Heating
4: MeMgI / diethyl ether / 24 h / Ambient temperature
With
hydrogenchloride; methyl magnesium iodide; aluminium trichloride; toluene-4-sulfonic acid; mercury; zinc;
In
diethyl ether; benzene;
DOI:10.1016/S0040-4020(01)96390-2
