(1R,5R)-ethyl 5-hydroxycyclohex-3-enecarboxylate

Base Information Edit

Chemical Name:(1R,5R)-ethyl 5-hydroxycyclohex-3-enecarboxylate
CAS No.:1287204-65-2
Molecular Formula:C₉H₁₄O₃
Molecular Weight:170.208
Hs Code.:
Mol file:1287204-65-2.mol

Synonyms:(1R,5R)-ethyl 5-hydroxycyclohex-3-enecarboxylate

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Chemical Property of (1R,5R)-ethyl 5-hydroxycyclohex-3-enecarboxylate Edit

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Technology Process of (1R,5R)-ethyl 5-hydroxycyclohex-3-enecarboxylate

There total 16 articles about (1R,5R)-ethyl 5-hydroxycyclohex-3-enecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 64-17-5
ethanol

: 109667-78-9
N-(4-chloro-7-oxo-6-oxabicyclo[3.2.1]octan-3-yl)acetamide

: 1287204-65-2
(1R,5R)-ethyl 5-hydroxycyclohex-3-enecarboxylate

Guidance literature:: With potassium carbonate; at 20 ℃; for 5h;
DOI:10.1016/j.tet.2011.01.064

Reference yield:

: ethyl 5-oxocyclohex-3-ene-1-carboxylate

: 1287204-65-2
(1R,5R)-ethyl 5-hydroxycyclohex-3-enecarboxylate

: 1266384-94-4
ethyl 5-hydroxycyclohex-3-enecarboxylate

: C₉H₁₆O₃

Guidance literature:: With glucose dehydrogenase; β-D-glucose; ketoreductase 105; nicotinamide adenine dinucleotide; magnesium sulfate; diothiothreitol; In aq. phosphate buffer; at 30 ℃; for 24h; pH=7; Enzymatic reaction;
DOI:10.1021/acs.joc.1c00326

Reference yield:

: ethyl 5-oxocyclohex-3-ene-1-carboxylate

: 1287204-65-2
(1R,5R)-ethyl 5-hydroxycyclohex-3-enecarboxylate

: C₉H₁₆O₃

Guidance literature:: With glucose dehydrogenase; β-D-glucose; ketoreductase 119; nicotinamide adenine dinucleotide; magnesium sulfate; diothiothreitol; In aq. phosphate buffer; at 30 ℃; for 24h; pH=7; Enzymatic reaction;
DOI:10.1021/acs.joc.1c00326