C₅H₃N(CH₂O(CH₂CH₂O)3C₆H₄OH)2

Base Information

• Chemical Name: C₅H₃N(CH₂O(CH₂CH₂O)3C₆H₄OH)2
• CAS No.: 947739-06-2
• Molecular Formula: C₃₁H₄₁NO₁₀
• Molecular Weight: 587.667
• Mol file: 947739-06-2.mol

Synonyms:C₅H₃N(CH₂O(CH₂CH₂O)3C₆H₄OH)2

Chemical Property of C₅H₃N(CH₂O(CH₂CH₂O)3C₆H₄OH)2

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅H₃N(CH₂O(CH₂CH₂O)3C₆H₄OH)2

There total 12 articles about C₅H₃N(CH₂O(CH₂CH₂O)3C₆H₄OH)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

C41H57NO12 → C5H3N(CH2O(CH2CH2O)3C6H4OH)2 (947739-06-2)

Guidance literature:

With hydrogenchloride; In methanol; at 20 ℃;

DOI:10.1039/b706527b

Reference yield: 99.0%

C41H57NO12 (947739-05-1) → C5H3N(CH2O(CH2CH2O)3C6H4OH)2 (947739-06-2)

Guidance literature:

With hydrogenchloride; In methanol; water; at 20 ℃;

DOI:10.1021/ic902265e

Reference yield:

C29H49NO10 → C5H3N(CH2O(CH2CH2O)3C6H4OH)2 (947739-06-2)

Guidance literature:

Multi-step reaction with 4 steps

1: 94 percent / aq. HCl / methanol / 20 °C

2: tetrahydrofuran / 20 °C

3: 83 percent / NaH / tetrahydrofuran / 72 h / Heating

4: 99 percent / aq. HCl / methanol / 20 °C

With hydrogenchloride; sodium hydride; In tetrahydrofuran; methanol;

DOI:10.1039/b706527b

upstream raw materials:

C₂₁H₃₇NO₁₂S₂

2.6-bis(hydroxymethyl)pyridine

2,6-bis(chloromethyl)pyridine

benzoate d'hydroxy-3 phenyle

Downstream raw materials:

[Sn(CC₄H₂N)4(C₆H₅)3(C₅H₄N)(C₅H₃N(CH₂O(CH₂CH₂O)3C₆H₄O)2)]

[Sn(meso-tetraphenylporphyrinato)((OC₆H₄(OC₂H₄)3OCH₂)2C₅H₃N)]

C₇₅H₆₃N₉O₁₀Sn

Refernces

• 1、 Guenet, Aurelie,Graf, Ernest,Kyritsakas, Nathalie,Allouche, Lionel,Hosseini, Mir Wais. "A molecular gate based on a porphyrin and a silver lock". . p. 2935 - 2937. Retrieved 2008/02/10.