ethyl 3,4-diacetoxycinnamate

Base Information

• Chemical Name: ethyl 3,4-diacetoxycinnamate
• CAS No.: 100976-84-9
• Molecular Formula: C₁₅H₁₆O₆
• Molecular Weight: 292.288
• Mol file: 100976-84-9.mol

Synonyms:ethyl 3,4-diacetoxycinnamate

Chemical Property of ethyl 3,4-diacetoxycinnamate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of ethyl 3,4-diacetoxycinnamate

There total 4 articles about ethyl 3,4-diacetoxycinnamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl caffeate (74257-25-3,102-37-4,66648-50-8) + acetic anhydride (108-24-7) + N-butylamine (109-73-9,85404-21-3) → ethyl 3,4-diacetoxycinnamate (100976-84-9) + diethyl-7-butyl-6,9,10-triacetoxybenz[k,l]acridine-1,2-dicarboxylate

Guidance literature:

ethyl caffeate; N-butylamine; With air; sodium hydrogencarbonate; sodium carbonate; In water; at 50 ℃; for 2h; pH=9.5;

With sodium tetrahydroborate;

acetic anhydride; With triethylamine;

DOI:10.1271/bbb.65.2121

Reference yield:

ethyl caffeate (74257-25-3,102-37-4,66648-50-8) + acetic anhydride (108-24-7) → ethyl 3,4-diacetoxycinnamate (100976-84-9)

Guidance literature:

With pyridine;

Reference yield:

vanillin (121-33-5,8014-42-4) → ethyl 3,4-diacetoxycinnamate (100976-84-9)

Guidance literature:

Multi-step reaction with 3 steps

1: PCl₅

2: aniline; piperidine

3: pyridine

With piperidine; pyridine; phosphorus pentachloride; aniline;

upstream raw materials:

ethyl caffeate

acetic anhydride

N-butylamine

vanillin

Downstream raw materials:

4-acetoxy-3-hydroxycinnamic acid ethyl ester

3-acetoxy-4-hydroxycinnamic acid ethyl ester

ethyl caffeate

methyl 3-(3,4-dihydroxyphenyl)propionate

Refernces