3-(4-CHLORO-BENZENESULFONYL)-PROPIONIC ACID

Base Information

• Chemical Name: 3-(4-CHLORO-BENZENESULFONYL)-PROPIONIC ACID
• CAS No.: 90396-00-2
• Molecular Formula: C9H9 Cl O4 S
• Molecular Weight: 248.687
• Hs Code.: 2916399090
• Mol file: 90396-00-2.mol

Synonyms:Propionicacid, 3-[(p-chlorophenyl)sulfonyl]- (6CI,7CI)

Chemical Property of 3-(4-CHLORO-BENZENESULFONYL)-PROPIONIC ACID

Chemical Property:

• Vapor Pressure: 5.3E-10mmHg at 25°C
• Boiling Point: 479.5°Cat760mmHg
• Flash Point: 243.8°C
• PSA: 79.82000
• Density: 1.455g/cm³
• LogP: 2.66920

Purity/Quality:

98%Min ^*data from raw suppliers

3-(4-Chloro-benzenesulfonyl)-propionic acid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-(4-CHLORO-BENZENESULFONYL)-PROPIONIC ACID

There total 7 articles about 3-(4-CHLORO-BENZENESULFONYL)-PROPIONIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

3-(4-chlorophenylsulfonyl)propanoyl chloride (932047-87-5) → p-chlorophenylsulfonylpropionic acid (90396-00-2)

Guidance literature:

aluminium trichloride; In carbon disulfide; for 3h; Ambient temperature;

Reference yield: 72.0%

3-[(4-chlorophenyl)sulfanyl]propanoic acid (6310-27-6) → p-chlorophenylsulfonylpropionic acid (90396-00-2)

Guidance literature:

With dihydrogen peroxide; In acetic acid;

Reference yield: 50.0%

3-(4-chlorophenylsulfonyl)propanoyl chloride (932047-87-5) → 6-chlorothiochroman-4-one 1,1-dioxide (90396-06-8) + p-chlorophenylsulfonylpropionic acid (90396-00-2)

Guidance literature:

aluminium trichloride; sulfuric acid; In carbon disulfide; at 25 - 90 ℃; for 4h;

upstream raw materials:

β-Propiolactone

4-chlorobenzenesulfinic acid

3-[(4-chlorophenyl)sulfanyl]propanoic acid

3-(4-chlorophenylsulfonyl)propanoyl chloride

Downstream raw materials:

3-(4-chlorophenylsulfonyl)propanoyl chloride

Refernces

• 1、 Abdel-Wahab, Aboel-Magd A.,El-Khawaga, Ahmed M.,El-Zohry, Maher F.,Khalaf, Ali A.. "MODERN FRIEDEL-CRAFTS CHEMISTRY. XI. CYCLIZATION OF ARYL HALOALKYL SULFONES, ARYLSULFONYLACYL CHLORIDES AND THEIR CORRESPONDING SULFIDES". . p. 31 - 44. Retrieved 2007/10/02.