Co(OC₆H₄CH₃)(P(C₆H₅)3)3

Base Information

• Chemical Name: Co(OC₆H₄CH₃)(P(C₆H₅)3)3
• CAS No.: 99668-72-1
• Molecular Formula: C₆₁H₅₂CoOP₃
• Molecular Weight: 952.998
• Mol file: 99668-72-1.mol

Synonyms:Co(OC₆H₄CH₃)(P(C₆H₅)3)3

Chemical Property of Co(OC₆H₄CH₃)(P(C₆H₅)3)3

Chemical Property:

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Technology Process of Co(OC₆H₄CH₃)(P(C₆H₅)3)3

There total 1 articles about Co(OC₆H₄CH₃)(P(C₆H₅)3)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

(PPh3)3CoH(N2) (21373-88-6,16920-54-0) + 1-acetoxy-4-methylbenzene (140-39-6) → HCo(CO)(P(C6H5)3)3 (53729-69-4,21329-67-9) + Co(OC6H4CH3)(P(C6H5)3)3 (99668-72-1) + methane (34557-54-5,27936-85-2) + nitrogen (7727-37-9) + hydrogen (1333-74-0)

Guidance literature:

In toluene; AcOC6H4Me added to CoH(N2)(PPh3)3 in toluene in vac., reacted for 3 days at room temp.; liquid phase analysed by GLC; hexane added, ppt. filtered, washed with hexane, dried in vac., recrystd. from C6H6-hexane;

DOI:10.1021/ja00263a007

upstream raw materials:

(PPh₃)3CoH(N₂)

1-acetoxy-4-methylbenzene

Refernces