tetrachloroacetone hydrate

Base Information

• Chemical Name: tetrachloroacetone hydrate
• CAS No.: 78950-58-0
• Molecular Formula: C₃H₄Cl₄O₂
• Molecular Weight: 213.876
• Mol file: 78950-58-0.mol

Synonyms:tetrachloroacetone hydrate

Chemical Property of tetrachloroacetone hydrate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of tetrachloroacetone hydrate

There total 11 articles about tetrachloroacetone hydrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

cis-Cyclooctene (931-88-4,931-87-3,25267-51-0) + 1,1,3,3-tetrachloropropanone (632-21-3) → Cyclooctene oxide (286-62-4) + tetrachloroacetone hydrate (78950-58-0)

Guidance literature:

With disodium hydrogenphosphate; dihydrogen peroxide; In chloroform; for 24h; Ambient temperature;

DOI:10.1016/S0040-4039(01)93284-8

Reference yield: 57.0%

2-methyl-2-pentene (625-27-4) + 1,1,3,3-tetrachloropropanone (632-21-3) → 2,3-epoxy-2-methylpentane (1192-22-9) + tetrachloroacetone hydrate (78950-58-0)

Guidance literature:

With disodium hydrogenphosphate; dihydrogen peroxide; In chloroform; for 24h; Ambient temperature;

DOI:10.1016/S0040-4039(01)93284-8

Reference yield: 56.0%

2-methylhept-1-ene (15870-10-7) + 1,1,3,3-tetrachloropropanone (632-21-3) → 2-methyl-2-pentyloxirane (53907-75-8,107608-96-8,140840-55-7,151284-11-6) + tetrachloroacetone hydrate (78950-58-0)

Guidance literature:

With disodium hydrogenphosphate; dihydrogen peroxide; In chloroform; for 24h; Ambient temperature;

DOI:10.1016/S0040-4039(01)93284-8

upstream raw materials:

2,4,4-trimethyl-1-pentene

1,1,3,3-tetrachloropropanone

cis-Cyclooctene

Cyclohex-2-enol

Downstream raw materials:

1,1,3,3-tetrachloropropanone

Refernces