Ethylazanium;chloride

Base Information

• Chemical Name: Ethylazanium;chloride
• CAS No.: 557-66-4
• Molecular Formula: C2H7N^.HCl
• Molecular Weight: 81.5452
• Hs Code.: 29211980
• Mol file: 557-66-4.mol

Synonyms:AKOS015892703

Chemical Property of Ethylazanium;chloride

Chemical Property:

• Appearance/Colour: white to off-white crystals
• Vapor Pressure: 1130mmHg at 25°C
• Melting Point: 107-108 °C(lit.)
• Refractive Index: 1.4202 (estimate)
• Boiling Point: 14.2 °C at 760 mmHg
• PSA: 26.02000
• Density: 1,22 g/cm3
• LogP: 1.46730
• Storage Temp.: Store below +30°C.
• Sensitive.: Hygroscopic
• Solubility.: soluble
• Water Solubility.: soluble
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 81.0345270
• Heavy Atom Count: 4
• Complexity: 2.8

Purity/Quality:

99% , ^*data from raw suppliers

Ethylamine Hydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36-37/39

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: CC[NH3+].[Cl-]
• Uses: Ethylamine Hydrochloride a chemical used in various chemical organic syntheses and biological studies. It is used in production of resins and rubber latex; also used in oil refining and organic syntheses.

Technology Process of Ethylazanium;chloride

There total 43 articles about Ethylazanium;chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

acetonitrile (75-05-8,26809-02-9) → ethanamine hydrochloride (557-66-4)

Guidance literature:

With hydrogenchloride; hydrogen; In propan-1-ol; water; at 60 - 70 ℃; for 18h; under 375.038 Torr; Flow reactor;

DOI:10.1002/open.201600166

Reference yield: 98.0%

N,N-bis(trimethylsilyl)ethanamine (2477-39-6) → Hexamethyldisiloxane (107-46-0) + ethanamine hydrochloride (557-66-4)

Guidance literature:

With hydrogenchloride;

Reference yield: 90.0%

bis(N-ethylsalicylaldiminato)nickel(II) (35968-61-7,13987-25-2,35672-82-3) + ammonium chloride → bis(N-salicylaldimino)nickel(II) (14283-99-9,36186-03-5) + ethanamine hydrochloride (557-66-4)

Guidance literature:

In methanol; stirring the soln. for 30 min between room temp. and 60°C, pptn.; filtration, washing with water, recrystn. from acetone;

DOI:10.1016/S0020-1693(00)83239-9

upstream raw materials:

N-chloroethylamine

N-ethyl-benzamidine; hydrochloride

diethyl ether

ethylamine

Downstream raw materials:

N-ethyl-N-(2-pyridin-2-ylethyl)amine

β-naphthol

4-ethylpiperazine

ethylamine-N-d2

Refernces

• 1、 -. "Green method for catalyzing reduction reaction of aliphatic nitro derivative". Paragraph 0005-0006; 0009-0012. . Retrieved 2021/07/31.
• 2、 Gudun, Kristina A.,Hayrapetyan, Davit,Khalimon, Andrey Y.,Segizbayev, Medet,Slamova, Ainur,Zakarina, Raikhan. "Cobalt-Catalyzed Deoxygenative Hydroboration of Nitro Compounds and Applications to One-Pot Synthesis of Aldimines and Amides". . . Retrieved 2021/11/30.