Technology Process of TIN (II) METHOXIDE
There total 13 articles about TIN (II) METHOXIDE which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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In
methanol;
byproducts: (C2H5)3SnCl; pptn. at dropwise addn. of a soln. of SnCl2 in CH3OH in an inert atmosphere (N2 or Ar) to a soln. of (C2H5)3SnOCH3 in CH3OH under stirring;; washing with CH3OH; drying in vac.;;
- Guidance literature:
-
In
methanol;
formation under exclusion of air and moisture by slow addn. of a methanolic SnBr2 soln. to a methanolic NaOCH3 soln.;; washing with CH3OH; drying in high vac. at 20°C;;
- Guidance literature:
-
In
methanol; benzene;
byproducts: Na(CH3C(O)CHC(O)CH3); N2 atmosphere; addn. of soln. of Sn(acac)2 in C6H6 to soln. of Na in MeOH (Sn : Na = 1 : 2, stirring, room temp.), stirring (0.5 h; pptn.); filtration, washing (MeOH, benzene), drying (vac.); elem. anal.;
DOI:10.1080/00945719708000227