N-Ethyl-Hexylamine

Base Information

• Chemical Name: N-Ethyl-Hexylamine
• CAS No.: 20352-67-4
• Molecular Formula: C8H19 N
• Molecular Weight: 129.24
• Hs Code.: 2921199090
• Mol file: 20352-67-4.mol

Synonyms:Hexylamine,N-ethyl- (6CI,8CI); Hexylethylamine; N-Ethylhexylamine

Chemical Property of N-Ethyl-Hexylamine

Chemical Property:

• Vapor Pressure: 2.1mmHg at 25°C
• Melting Point: -66°C (estimate)
• Refractive Index: 1.4187
• Boiling Point: 163°C at 760 mmHg
• Flash Point: 39.7°C
• PSA: 12.03000
• Density: 0.762g/cm³
• LogP: 2.56710

Purity/Quality:

98%min ^*data from raw suppliers

N-Ethyl-hexylamine >98 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-Ethyl-Hexylamine

There total 19 articles about N-Ethyl-Hexylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

ethanol (64-17-5) + hexan-1-amine (111-26-2) → N-ethylhexylamine (20352-67-4)

Guidance literature:

With Zr₆O₄(OH)₄(BDC-NH₂)_5.7([LIr]BF₄)_0.3; at 80 ℃; for 2h; Catalytic behavior; Autoclave; Green chemistry;

DOI:10.1002/cctc.201402101

Reference yield: 89.0%

triethyl borane (97-94-9) + N-benzoyloxy-hexylamine (220645-25-0) → N-ethylhexylamine (20352-67-4)

Guidance literature:

With sodium carbonate; In tetrahydrofuran; 0 deg C to reflux;

DOI:10.1021/jo981613l

Reference yield: 82.0%

N-hexylacetamide (7501-79-3) → N-ethylhexylamine (20352-67-4)

Guidance literature:

With hydrogen; hexarhodium hexadecacarbonyl; decacarbonyldirhenium⁽⁰⁾; In 1,2-dimethoxyethane; at 170 ℃; for 16h; under 76000 Torr;

DOI:10.1016/S0040-4039(96)01458-X

upstream raw materials:

ethene

hexan-1-amine

ethyl-benzyl-hexyl-amine

O-ethyl O-phenyl methylphosphonate

Refernces

• 1、 Matzel, Philipp,Wenske, Sebastian,Merdivan, Simon,Günther, Sebastian,H?hne, Matthias. "Synthesis of β-Chiral Amines by Dynamic Kinetic Resolution of α-Branched Aldehydes Applying Imine Reductases". . p. 4281 - 4285. Retrieved 2019/08/20.
• 2、 Stein, Mario,Breit, Bernhard. "Catalytic hydrogenation of amides to amines under mild conditions". supporting information. p. 2231 - 2234. Retrieved 2013/03/28.