ethylmagnesium iodide

Base Information

• Chemical Name: ethylmagnesium iodide
• CAS No.: 10467-10-4
• Molecular Formula: C2H5 I Mg
• Molecular Weight: 180.271
• Hs Code.: 2931900090
• Mol file: 10467-10-4.mol

Synonyms:Ethylmagnesiumiodide (6CI); Ethyliodomagnesium; Ethylmagnesium iodine

Chemical Property of ethylmagnesium iodide

Chemical Property:

• PSA: 0.00000
• LogP: 1.85960

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s): 3
• Hazard Codes: 3:
• Safety Statements: Mixtures with ethoxyacetylene in ether are explosive. When heated to decomposition it emits toxic fumes of I:

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ethylmagnesium iodide

There total 4 articles about ethylmagnesium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diethyl ether (60-29-7,927820-24-4) + iodine (7553-56-2,12190-71-5,8031-47-8) + hexaethyl diplumbane (2388-00-3) + benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → ethylmagnesium iodide (10467-10-4) + tetraethyllead(IV) (78-00-2)

Guidance literature:

DOI:10.1021/ja01872a053

Reference yield:

Ag(0-74.5),Mg(b) (W%) + ethyl iodide (75-03-6) → ethylmagnesium iodide (10467-10-4) + silver (7440-22-4)

Guidance literature:

In diethyl ether; dry powdered alloy, N2-atmosphere, residue is pure silver; reactivity deepnding on Mg-content;;

Reference yield:

→ ethylmagnesium iodide (10467-10-4) + 2-[4-chloro-4-(2-chloro-2-ethoxycarbonylethenyl)phenyl]-3-ethyl-3-hydroxy-2,3,4,5,6,7-hexahydroisoindol-1-one

Guidance literature:

upstream raw materials:

diethyl ether

iodine

hexaethyl diplumbane

benzene

Downstream raw materials:

butanone

3-Phenylpropenol

1-phenyl-pent-1-en-3-one

3-phenylpentan-3-ol

Refernces

• 1、 -. "Piperazinobutyrophenone derivatives". . . Retrieved 2008/06/13.