β-phenylisovaleryl p-nitrobenzoyl peroxide

Base Information

• Chemical Name: β-phenylisovaleryl p-nitrobenzoyl peroxide
• CAS No.: 51380-79-1
• Molecular Formula: C₁₈H₁₇NO₆
• Molecular Weight: 343.336
• Mol file: 51380-79-1.mol

Synonyms:β-phenylisovaleryl p-nitrobenzoyl peroxide

Chemical Property of β-phenylisovaleryl p-nitrobenzoyl peroxide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of β-phenylisovaleryl p-nitrobenzoyl peroxide

There total 2 articles about β-phenylisovaleryl p-nitrobenzoyl peroxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-nitroperbenzoic acid (943-39-5) + 3-methyl-3-phenyl-butyryl chloride (4094-64-8) → β-phenylisovaleryl p-nitrobenzoyl peroxide (51380-79-1)

Guidance literature:

DOI:10.1021/ja00416a013

Reference yield:

→ β-phenylisovaleryl p-nitrobenzoyl peroxide (51380-79-1)

Guidance literature:

Saeurechlorid v.6c, p-Nitroperoxybenzoesaeure;

DOI:10.1021/jo00928a027

Reference yield: 92.8%

β-phenylisovaleryl p-nitrobenzoyl peroxide (51380-79-1) → 4,4-dimethyl-2-oxo-chroman (29598-22-9) + 2-Methyl-1-phenyl-2-propanol (100-86-7) + (2-methyl-1-propenyl)-benzene (768-49-0) + 3-phenylbut-1-ene (934-10-1) + 2-phenylbut-2-ene (767-99-7,768-00-3,2082-61-3) + 4-nitro-benzoic acid (62-23-7)

Guidance literature:

With P₀ silica; at 40 ℃; Rate constant; reactions without P₀ silica in cyclohexane at the various temperatures;

DOI:10.1021/ja00416a013

upstream raw materials:

4-nitroperbenzoic acid

3-methyl-3-phenyl-butyryl chloride

Downstream raw materials:

4,4-dimethyl-2-oxo-chroman

2-Methyl-1-phenyl-2-propanol

(2-methyl-1-propenyl)-benzene

3-phenylbut-1-ene

Refernces