10-Diazonioanthracen-9-olate

Base Information

• Chemical Name: 10-Diazonioanthracen-9-olate
• CAS No.: 1705-82-4
• Molecular Formula: C14H8 N2 O
• Molecular Weight: 220.23
• Hs Code.: 2927000090
• ChEMBL ID: CHEMBL65889
• DSSTox Substance ID: DTXSID80401612
• Nikkaji Number: J1.365.064K
• Wikidata: Q82204812
• Mol file: 1705-82-4.mol

Synonyms:10-diazonioanthracen-9-olate;1705-82-4;9(10H)-Anthracenone, 10-diazo-;10-Diazo-9-anthrone;diazoanthrone;CHEMBL65889;SCHEMBL8936666;DTXSID80401612;AKOS024331491;FT-0607187

Chemical Property of 10-Diazonioanthracen-9-olate

Chemical Property:

• PSA: 54.46000
• LogP: 2.37926
• XLogP3: 5.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 0
• Exact Mass: 220.063662883
• Heavy Atom Count: 17
• Complexity: 310

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C2C(=C1)C(=C3C=CC=CC3=C2[O-])[N+]#N

Technology Process of 10-Diazonioanthracen-9-olate

There total 1 articles about 10-Diazonioanthracen-9-olate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

anthracen-9(10H)-one (90-44-8) → 10-diazo-10H-anthracen-9-one (1705-82-4) + 9,10-phenanthrenequinone (84-65-1)

Guidance literature:

With 15-crown-5; 2-azido-1,3-dimethylimidazolinium chloride; triethylamine; In tetrahydrofuran; acetonitrile; at -20 ℃; for 0.166667h;

DOI:10.1055/s-0030-1258568

Reference yield: 97.0%

10-diazo-10H-anthracen-9-one (1705-82-4) + isopropenylbenzene (98-83-9,6144-04-3,25014-31-7,42612-14-6) → C23H18O (34874-43-6)

Guidance literature:

In benzene; Irradiation;

DOI:10.1021/jo00252a023

Reference yield: 87.0%

4-Phenyl-1,2,4-triazolidine-3,5-dione (4233-33-4) + 10-diazo-10H-anthracen-9-one (1705-82-4) → 2-(9,10-Dihydro-10-oxo-9-anthracenylio)-3,5-dioxo-4-phenyl-1,2,4-triazolidin-1-id (79536-75-7)

Guidance literature:

In benzene; for 5h; Ambient temperature;

upstream raw materials:

anthracen-9(10H)-one

Downstream raw materials:

2',2'-diphenylspiro-10-one

2-(9,10-Dihydro-10-oxo-9-anthracenylio)-3,5-dioxo-4-phenyl-1,2,4-triazolidin-1-id

anthracen-9(10H)-one

bianthronyl

Refernces