diphenyl phenylphosphoramidite

Base Information

• Chemical Name: diphenyl phenylphosphoramidite
• CAS No.: 26350-10-7
• Molecular Formula: C₁₈H₁₆NO₂P
• Molecular Weight: 309.304
• Mol file: 26350-10-7.mol

Synonyms:diphenyl phenylphosphoramidite

Chemical Property of diphenyl phenylphosphoramidite

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of diphenyl phenylphosphoramidite

There total 1 articles about diphenyl phenylphosphoramidite which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.5%

N,N,N’,N’-tetraethyl-P-phenyl-phosphonic diamide (4519-35-1) + aniline (62-53-3) → triphenyl phosphite (101-02-0) + N,N',N''-triphenylphosphorous triamide (15159-51-0) + phenyl N,N'-diphenylphosphorodiamidite (26350-11-8) + diphenyl phenylphosphoramidite (26350-10-7) + diethylamine (109-89-7)

Guidance literature:

for 17h; Product distribution; Heating;

Reference yield:

diphenyl phenylphosphoramidite (26350-10-7) → N-(hexafluoroisopropylidene)aniline (2002-95-1)

Guidance literature:

Multi-step reaction with 2 steps

1: CH₂Cl₂ / -78 °C

2: 150 °C

In dichloromethane;

DOI:10.1039/P19730000972

Reference yield:

diphenyl phenylphosphoramidite (26350-10-7) → 1,1,1,3,3,3-hexafluoropropan-2-yl diphenyl phosphate (22410-38-4)

Guidance literature:

Multi-step reaction with 2 steps

1: CH₂Cl₂ / -78 °C

2: 150 °C

In dichloromethane;

DOI:10.1039/P19730000972

upstream raw materials:

N,N,N’,N’-tetraethyl-P-phenyl-phosphonic diamide

aniline

Downstream raw materials:

(1-phenoxy-cyclohexyl)-phosphonic acid anilide-phenyl ester

N-(hexafluoroisopropylidene)aniline

1,1,1,3,3,3-hexafluoropropan-2-yl diphenyl phosphate

phenyl-amidophosphoric acid diphenyl ester

Refernces