Technology Process of C44H48N4O11
There total 4 articles about C44H48N4O11 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
trifluoroacetic acid;
In
dichloromethane;
at 20 ℃;
for 5h;
Inert atmosphere;
DOI:10.1016/j.tet.2012.02.040
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: palladium on activated charcoal; ammonium formate / methanol / 20 °C
1.2: -15 - 20 °C
1.3: 20 °C
2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 20 °C
3.1: trifluoroacetic acid / dichloromethane / 20 °C
With
palladium on activated charcoal; ammonium formate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid;
In
methanol; dichloromethane;
DOI:10.1016/j.chemphyslip.2019.104832
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 20 °C
2: trifluoroacetic acid / dichloromethane / 20 °C
With
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid;
In
dichloromethane;
DOI:10.1016/j.chemphyslip.2019.104832