C₃₄H₄₅NO₁₁

Base Information

• Chemical Name: C₃₄H₄₅NO₁₁
• CAS No.: 639-24-7
• Molecular Formula: C₃₄H₄₅NO₁₁
• Molecular Weight: 643.731
• Mol file: 639-24-7.mol

Synonyms:C₃₄H₄₅NO₁₁

Chemical Property of C₃₄H₄₅NO₁₁

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₄H₄₅NO₁₁

There total 1 articles about C₃₄H₄₅NO₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

indaconitine (302-27-2,140188-61-0) → C33H41NO10 + C34H45NO11 (639-24-7)

Guidance literature:

With Jones reagent; In acetone; at 0 ℃; for 0.5h;

DOI:10.1080/10286020.2012.684684

Reference yield: 12.0%

C34H45NO11 (639-24-7) → indaconitine (302-27-2,140188-61-0) + aconitine

Guidance literature:

With sodium tetrahydroborate; In methanol; at 20 ℃; for 12h;

DOI:10.1080/10286020.2012.684684

Reference yield:

C34H45NO11 (639-24-7) → 3,13,15-O-triacetylaconitine (67806-02-4)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol / 12 h / 20 °C

2: toluene-4-sulfonic acid / 48 h / 20 °C

With sodium tetrahydroborate; toluene-4-sulfonic acid; In methanol;

DOI:10.1080/10286020.2012.684684

upstream raw materials:

indaconitine

Downstream raw materials:

3,13,15-O-triacetylaconitine

pyroaconitine

C₂₅H₄₁NO₈

C₃₂H₄₅NO₉

Refernces