C₃₅H₃₈N₂O₉S

Base Information

• Chemical Name: C₃₅H₃₈N₂O₉S
• CAS No.: 1429056-90-5
• Molecular Formula: C₃₅H₃₈N₂O₉S
• Molecular Weight: 662.761
• Mol file: 1429056-90-5.mol

Synonyms:C₃₅H₃₈N₂O₉S

Chemical Property of C₃₅H₃₈N₂O₉S

Chemical Property:

Purity/Quality:

Safty Information:

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• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₅H₃₈N₂O₉S

There total 2 articles about C₃₅H₃₈N₂O₉S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

C47H62N2O9S (1429056-89-2) → C35H38N2O9S (1429056-90-5)

Guidance literature:

With formic acid; at 20 ℃;

DOI:10.1016/j.carres.2013.01.023

Reference yield:

Nα-Fmoc-S-benzylcysteine (53298-33-2,252049-18-6) + 4-amino-4-(2-tert-butoxycarbonylethyl)heptanedioic acid di-tertbutyl ester (136586-99-7) → C35H38N2O9S (1429056-90-5)

Guidance literature:

Multi-step reaction with 2 steps

1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C

2: formic acid / 20 °C

With formic acid; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;

DOI:10.1016/j.carres.2013.01.023

Reference yield: 62.0%

C35H38N2O9S (1429056-90-5) + 2-azidoethyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside (140428-83-7) → C83H107N5O36S

Guidance literature:

With tributylphosphine; DIC; benzotriazol-1-ol; In tetrahydrofuran; at 0 - 20 ℃; for 40h; Inert atmosphere; Schlenk technique;

DOI:10.1016/j.carres.2013.01.023

upstream raw materials:

N^α-Fmoc-S-benzylcysteine

4-amino-4-(2-tert-butoxycarbonylethyl)heptanedioic acid di-tertbutyl ester

C₄₇H₆₂N₂O₉S

Refernces