diisopropylammonium (Z)-3-phenylacrylate

Base Information

• Chemical Name: diisopropylammonium (Z)-3-phenylacrylate
• CAS No.: 1265912-86-4
• Molecular Formula: C₆H₁₅N*C₉H₈O₂
• Molecular Weight: 249.353
• Mol file: 1265912-86-4.mol

Synonyms:diisopropylammonium (Z)-3-phenylacrylate

Chemical Property of diisopropylammonium (Z)-3-phenylacrylate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of diisopropylammonium (Z)-3-phenylacrylate

There total 1 articles about diisopropylammonium (Z)-3-phenylacrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

Cinnamic acid (621-82-9) + diisopropylamine (108-18-9) → diisopropylammonium (Z)-3-phenylacrylate (1265912-86-4)

Guidance literature:

In diethyl ether; at 20 ℃;

DOI:10.1021/jm1011676

Reference yield: 95.0%

diisopropylammonium (Z)-3-phenylacrylate (1265912-86-4) → cis-cinnamic acid (140-10-3,621-82-9,102-94-3)

Guidance literature:

With hydrogenchloride; In water;

DOI:10.1021/jm1011676

Reference yield:

diisopropylammonium (Z)-3-phenylacrylate (1265912-86-4) → (Z)-1-((1S,5R)-5-(3-methoxyphenyl)-2-azabicyclo[3.3.1]nonan-2-yl)-3-phenylprop-2-en-1-one (1265912-67-1)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrogenchloride / water

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

With hydrogenchloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; water;

DOI:10.1021/jm1011676

upstream raw materials:

Cinnamic acid

diisopropylamine

Downstream raw materials:

(Z)-1-((1S,5R)-5-(3-methoxyphenyl)-2-azabicyclo[3.3.1]nonan-2-yl)-3-phenylprop-2-en-1-one

(Z)-1-((1R,5S)-5-(3-methoxyphenyl)-2-azabicyclo[3.3.1]nonan-2-yl)-3-phenylprop-2-en-1-one

(Z)-1-((1S,5R)-5-(3-hydroxyphenyl)-2-azabicyclo[3.3.1]nonan-2-yl)-3-phenylprop-2-en-1-one

(Z)-1-((1R,5S)-5-(3-hydroxyphenyl)-2-azabicyclo[3.3.1]nonan-2-yl)-3-phenylprop-2-en-1-one

Refernces