Technology Process of methyl(diphenyl)gallium
There total 2 articles about methyl(diphenyl)gallium which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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In
neat (no solvent);
(CH3)3Ga was added to freshly sublimed diphenylmercury, the suspn. was heated at 100°C in a closed vessel for 3 h, cooled to room temp. without stiring; volatiles were removed in vac. (1E-2 mbar), crystals were washed with n-hexane and dried in vac. for 2 h: elem. anal.;
DOI:10.1021/om701055a
- Guidance literature:
-
In
neat (no solvent);
(C6H5)Ga(CH3)2 was evacuated into a Schlenk flask, heated to 70, 120 and150°C each for a period of 30 min; not sepd., detected by NMR spectra;
DOI:10.1021/om701055a
- Guidance literature:
-
In
neat (no solvent);
(C6H5)Ga(CH3)2 was evacuated into a Schlenk flask, heated to 150°C for 30 min; not sepd., detected by NMR spectra;
DOI:10.1021/om701055a
