Technology Process of C37H23N
There total 5 articles about C37H23N which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); sodium hydrogencarbonate;
In
ethanol; water; toluene;
at 80 ℃;
for 16h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetrakis(triphenylphosphine) palladium(0); caesium carbonate / acetonitrile; tetrahydrofuran; N,N-dimethyl acetamide / 18 h / 75 °C / Inert atmosphere
2: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; 1,1'-bis(diphenylphosphino)ferrocene; potassium acetate / dimethyl sulfoxide / 14 h / 100 °C / Inert atmosphere
3: tetrakis(triphenylphosphine) palladium(0); sodium hydrogencarbonate / ethanol; toluene; water / 16 h / 80 °C / Inert atmosphere
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium(0); 1,1'-bis(diphenylphosphino)ferrocene; potassium acetate; sodium hydrogencarbonate; caesium carbonate;
In
tetrahydrofuran; ethanol; N,N-dimethyl acetamide; water; dimethyl sulfoxide; toluene; acetonitrile;
1: |Suzuki Coupling;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetrakis(triphenylphosphine) palladium(0); caesium carbonate / acetonitrile; tetrahydrofuran; N,N-dimethyl acetamide / 18 h / 75 °C / Inert atmosphere
2: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; 1,1'-bis(diphenylphosphino)ferrocene; potassium acetate / dimethyl sulfoxide / 14 h / 100 °C / Inert atmosphere
3: tetrakis(triphenylphosphine) palladium(0); sodium hydrogencarbonate / ethanol; toluene; water / 16 h / 80 °C / Inert atmosphere
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium(0); 1,1'-bis(diphenylphosphino)ferrocene; potassium acetate; sodium hydrogencarbonate; caesium carbonate;
In
tetrahydrofuran; ethanol; N,N-dimethyl acetamide; water; dimethyl sulfoxide; toluene; acetonitrile;
1: |Suzuki Coupling;