C₃₆H₃₀N₁₂O₁₂S₄

Base Information

• Chemical Name: C₃₆H₃₀N₁₂O₁₂S₄
• CAS No.: 1375454-23-1
• Molecular Formula: C₃₆H₃₀N₁₂O₁₂S₄
• Molecular Weight: 950.971
• Mol file: 1375454-23-1.mol

Synonyms:C₃₆H₃₀N₁₂O₁₂S₄

Chemical Property of C₃₆H₃₀N₁₂O₁₂S₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₆H₃₀N₁₂O₁₂S₄

There total 2 articles about C₃₆H₃₀N₁₂O₁₂S₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-amino-1-benzenesulfonic acid (88-21-1) + C24H22N8O6S2 (19586-68-6) → C36H30N12O12S4 (1375454-23-1)

Guidance literature:

2-amino-1-benzenesulfonic acid; With lithium hydroxide; In water; pH=< 11;

With hydrogenchloride; sodium nitrite; In water; at 5 - 10 ℃; for 0.75h; pH=< 0.8;

C₂₄H₂₂N₈O₆S₂; With sodium carbonate; In water; at 20 ℃; for 1.5h; pH=8 - 8.2;

Reference yield:

4,4'-diamino-2,2'-biphenyldisulfonic acid (117-61-3) + m-phenylenediamine (108-45-2,64554-26-3,76583-20-5) → C36H30N12O12S4 (1375454-23-1)

Guidance literature:

Multi-step reaction with 2 steps

1.1: hydrogenchloride; sodium nitrite; lithium hydroxide / water / 3.5 h / -5 - 20 °C / pH 11.5

1.2: 3.25 h / 20 °C / pH 8 - 10.6

2.1: hydrogenchloride; sodium nitrite; lithium hydroxide / water / 0.75 h / 5 - 20 °C / pH < 11 / Cooling

2.2: 1.83 h / 20 °C / pH 8 - 8.2

2.3: 1 h

With hydrogenchloride; lithium hydroxide; sodium nitrite; In water;

upstream raw materials:

2-amino-1-benzenesulfonic acid

C₂₄H₂₂N₈O₆S₂

4,4'-diamino-2,2'-biphenyldisulfonic acid

m-phenylenediamine

Refernces

• 1、 -. "AZO DYES". Page/Page column 28-29. . Retrieved 2012/06/16.