Ethanone, 1-(4-hydroxyphenyl)-, hydrazone

Base Information

• Chemical Name: Ethanone, 1-(4-hydroxyphenyl)-, hydrazone
• CAS No.: 805233-94-7
• Molecular Formula: C8H10 N2 O
• Molecular Weight: 150.18
• Mol file: 805233-94-7.mol

Synonyms:4'-Hydroxyacetophenonehydrazone

Chemical Property of Ethanone, 1-(4-hydroxyphenyl)-, hydrazone

Chemical Property:

• PSA: 58.61000
• LogP: 1.77520

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Ethanone, 1-(4-hydroxyphenyl)-, hydrazone

There total 6 articles about Ethanone, 1-(4-hydroxyphenyl)-, hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-Hydroxyacetophenone (99-93-4) → 1-(4-hydroxy-phenyl)-ethanone-hydrazone (805233-94-7)

Guidance literature:

With hydrazine hydrate;

Reference yield:

2-dimethylamino-1-(4-hydroxy-phenyl)-ethanone (189506-44-3) → 1-(4-hydroxy-phenyl)-ethanone-hydrazone (805233-94-7)

Guidance literature:

With water; hydrazine hydrate;

DOI:10.1021/ja01123a013

Reference yield:

p-hydroxyphenacyl chloride (6305-04-0) → 1-(4-hydroxy-phenyl)-ethanone-hydrazone (805233-94-7)

Guidance literature:

Multi-step reaction with 2 steps

1: NaI; acetone / anschliessendes Behandeln mit Dimethylamin in Aether

2: water; N₂H₄+H₂O

With water; hydrazine hydrate; acetone; sodium iodide;

DOI:10.1021/ja01123a013

upstream raw materials:

2-dimethylamino-1-(4-hydroxy-phenyl)-ethanone

4-Hydroxyacetophenone

4-Hydroxyacetophenone N,N-dimethylhydrazone

water

Downstream raw materials:

4-acetaminophenol

4-Ethylphenol

Refernces