Technology Process of CIS-1,4-DIBENZYLOXY-2-BUTENE
There total 15 articles about CIS-1,4-DIBENZYLOXY-2-BUTENE which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium hydroxide; triethylbenzyl ammonium bromide;
In
dichloromethane;
for 2.5h;
Ambient temperature;
- Guidance literature:
-
1,4-butenediol;
With
sodium hydride;
In
N,N-dimethyl-formamide; mineral oil;
at 0 - 20 ℃;
for 1h;
benzyl bromide;
In
N,N-dimethyl-formamide; mineral oil;
at 20 ℃;
for 4h;
DOI:10.1016/j.tet.2010.11.038
- Guidance literature:
-
With
copper; ethylene glycol; potassium hydroxide;
at 150 ℃;
for 0.5h;
stereoselective reaction;
Sonication;
Microwave irradiation;
Green chemistry;
DOI:10.1002/adsc.202100126