C₃₂H₁₈O₂

Base Information

• Chemical Name: C₃₂H₁₈O₂
• CAS No.: 1352791-03-7
• Molecular Formula: C₃₂H₁₈O₂
• Molecular Weight: 434.494
• Mol file: 1352791-03-7.mol

Synonyms:

Chemical Property of C₃₂H₁₈O₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of C₃₂H₁₈O₂

There total 1 articles about C₃₂H₁₈O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

2,8-dibromo-indeno[1,2-b]fluorene-6,12-dione (853234-57-8) + phenylboronic acid (98-80-6) → C32H18O2 (1352791-03-7)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In water; toluene; for 48h; Inert atmosphere; Reflux;

DOI:10.1002/anie.201104797

Reference yield:

C32H18O2 (1352791-03-7) + tris-iso-propylsilyl acetylene (89343-06-6) → C54H62O2Si2 (1352800-80-6)

Guidance literature:

tris-iso-propylsilyl acetylene; With n-butyllithium; In tetrahydrofuran; at 0 ℃; for 0.333333h; Inert atmosphere;

C₃₂H₁₈O₂; In tetrahydrofuran; at 20 ℃; for 2h; Cooling; Inert atmosphere;

DOI:10.1002/anie.201104797

upstream raw materials:

2,8-dibromo-indeno[1,2-b]fluorene-6,12-dione

phenylboronic acid

Downstream raw materials:

C₅₄H₆₂O₂Si₂

Refernces