Os(C₁₀H₈N₂)2((C₁₀H₈N₂)(CH₂)3)Cl⁽¹⁺⁾*PF₆^(1-)=[Os(C₁₀H₈N₂)2((C₁₀H₈N₂)(CH₂)3)Cl]PF₆

Base Information

• Chemical Name: Os(C₁₀H₈N₂)2((C₁₀H₈N₂)(CH₂)3)Cl⁽¹⁺⁾*PF₆^(1-)=[Os(C₁₀H₈N₂)2((C₁₀H₈N₂)(CH₂)3)Cl]PF₆
• CAS No.: 133793-82-5
• Molecular Formula: C₃₃H₃₀ClN₆Os*F₆P
• Molecular Weight: 881.259
• Mol file: 133793-82-5.mol

Synonyms:

Chemical Property of Os(C₁₀H₈N₂)2((C₁₀H₈N₂)(CH₂)3)Cl⁽¹⁺⁾*PF₆^(1-)=[Os(C₁₀H₈N₂)2((C₁₀H₈N₂)(CH₂)3)Cl]PF₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Os(C₁₀H₈N₂)2((C₁₀H₈N₂)(CH₂)3)Cl⁽¹⁺⁾*PF₆^(1-)=[Os(C₁₀H₈N₂)2((C₁₀H₈N₂)(CH₂)3)Cl]PF₆

There total 1 articles about Os(C₁₀H₈N₂)2((C₁₀H₈N₂)(CH₂)3)Cl⁽¹⁺⁾*PF₆^(1-)=[Os(C₁₀H₈N₂)2((C₁₀H₈N₂)(CH₂)3)Cl]PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bis(2,2'-bipyridine)osmium(II) dichloride (15702-72-4,79982-56-2) + 1,3-di(4-pyridyl)propane (17252-51-6) → Os(C10H8N2)2((C10H8N2)(CH2)3)Cl(1+)*PF6(1-)=[Os(C10H8N2)2((C10H8N2)(CH2)3)Cl]PF6 (133793-82-5,155888-48-5,136655-29-3)

Guidance literature:

In ethylene glycol; soln. of Os-compd. was refluxed with 2 equiv. 4,4'-trimethylenedipyridine for 3h under N2; cooled, equiv. water was added, filtd., satd. aq. soln. of NH4PF6 was added, collected, washed with water, dried with ether, cromd. on alumina with 15% MeOH in toluene;

DOI:10.1021/j100176a098

upstream raw materials:

bis(2,2'-bipyridine)osmium(II) dichloride

1,3-di(4-pyridyl)propane

Refernces