C₁₄H₁₇N

Base Information

• Chemical Name: C₁₄H₁₇N
• CAS No.: 1260147-07-6
• Molecular Formula: C₁₄H₁₇N
• Molecular Weight: 199.296
• Mol file: 1260147-07-6.mol

Synonyms:

Chemical Property of C₁₄H₁₇N

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of C₁₄H₁₇N

There total 2 articles about C₁₄H₁₇N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-ethyl-1,5-dimethylpyrrole (90154-79-3) + [Ph2I]BF4 → C14H17N (1260147-07-6) + C14H17N (1260147-23-6)

Guidance literature:

2-ethyl-1,5-dimethylpyrrole; With dichloro bis(acetonitrile) palladium(II); In 1,2-dichloro-ethane; at 20 ℃; for 0.0833333h;

[Ph₂I]BF₄; In 1,2-dichloro-ethane; at 84 ℃; for 2h;

DOI:10.1021/ol102734g

Reference yield:

heptane-2,5-dione (1703-51-1) → C14H17N (1260147-07-6) + C14H17N (1260147-23-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: aminosulfonic acid / ethanol

2.1: dichloro bis(acetonitrile) palladium(II) / 1,2-dichloro-ethane / 0.08 h / 20 °C

2.2: 2 h / 84 °C

With dichloro bis(acetonitrile) palladium(II); aminosulfonic acid; In ethanol; 1,2-dichloro-ethane; 1.1: Paal-Knorr reaction;

DOI:10.1021/ol102734g

upstream raw materials:

2-ethyl-1,5-dimethylpyrrole

heptane-2,5-dione

Refernces