Technology Process of 4-(4'-pyridyl)phenyl 4''-n-hexyloxybenzoate
There total 5 articles about 4-(4'-pyridyl)phenyl 4''-n-hexyloxybenzoate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) NaNO2, HCl / 2.) 40 deg C, 3 h
2: 89 percent / 95percent hydrazine hydrate / 5percent Pd/C / ethanol / 1.5 h / Heating
3: 1.) NaNO2, HCl / 1.) H2O, 2.) H2O, 60-90 deg C, 3 h, 3.) purification via picrate salt
4: pyridine
With
pyridine; hydrogenchloride; hydrazine hydrate; sodium nitrite;
palladium on activated charcoal;
In
ethanol;
DOI:10.1080/15421408008084013
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 89 percent / 95percent hydrazine hydrate / 5percent Pd/C / ethanol / 1.5 h / Heating
2: 1.) NaNO2, HCl / 1.) H2O, 2.) H2O, 60-90 deg C, 3 h, 3.) purification via picrate salt
3: pyridine
With
pyridine; hydrogenchloride; hydrazine hydrate; sodium nitrite;
palladium on activated charcoal;
In
ethanol;
DOI:10.1080/15421408008084013
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) NaNO2, HCl / 2.) 40 deg C, 3 h
2: 89 percent / 95percent hydrazine hydrate / 5percent Pd/C / ethanol / 1.5 h / Heating
3: 1.) NaNO2, HCl / 1.) H2O, 2.) H2O, 60-90 deg C, 3 h, 3.) purification via picrate salt
4: pyridine
With
pyridine; hydrogenchloride; hydrazine hydrate; sodium nitrite;
palladium on activated charcoal;
In
ethanol;
DOI:10.1080/15421408008084013
