1-Anilino-2.2.2-trichlor-ethyl-carbaminsaeureethylester

Base Information

• Chemical Name: 1-Anilino-2.2.2-trichlor-ethyl-carbaminsaeureethylester
• CAS No.: 16723-33-4
• Molecular Formula: C₁₁H₁₃Cl₃N₂O₂
• Molecular Weight: 311.595
• Mol file: 16723-33-4.mol

Synonyms:

Chemical Property of 1-Anilino-2.2.2-trichlor-ethyl-carbaminsaeureethylester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-Anilino-2.2.2-trichlor-ethyl-carbaminsaeureethylester

There total 4 articles about 1-Anilino-2.2.2-trichlor-ethyl-carbaminsaeureethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2,2,2-trichloro-ethylidene)-carbamic acid ethyl ester (16723-30-1) → 1-Anilino-2.2.2-trichlor-ethyl-carbaminsaeureethylester (16723-33-4)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂O / acetone

2: triethylenediamine / benzene

With 1,4-diaza-bicyclo[2.2.2]octane; water; In acetone; benzene;

DOI:10.1021/jo01271a061

Reference yield:

(2,2,2-trichloro-1-hydroxy-ethyl)-carbamic acid ethyl ester (541-79-7) → 1-Anilino-2.2.2-trichlor-ethyl-carbaminsaeureethylester (16723-33-4)

Guidance literature:

Multi-step reaction with 3 steps

1: SOCl₂, Py / CH₂Cl₂

2: Et₃N / benzene

3: CCl₄

With pyridine; thionyl chloride; triethylamine; In tetrachloromethane; dichloromethane; benzene;

DOI:10.1021/jo01271a061

Reference yield:

(1,2,2,2-tetrachloro-ethyl)-carbamic acid ethyl ester (3659-12-9) → 1-Anilino-2.2.2-trichlor-ethyl-carbaminsaeureethylester (16723-33-4)

Guidance literature:

Multi-step reaction with 2 steps

1: Et₃N / benzene

2: CCl₄

With triethylamine; In tetrachloromethane; benzene;

DOI:10.1021/jo01271a061

upstream raw materials:

(1,2,2,2-tetrachloro-ethyl)-carbamic acid ethyl ester

aniline

(2,2,2-trichloro-ethylidene)-carbamic acid ethyl ester

(2,2,2-trichloro-1-hydroxy-ethyl)-carbamic acid ethyl ester