Co₄O(O₂CC(CH₃)3)4(C₆H₅N₂C₇H₄C₄H₂NC₇H₄N₂C₆H₅)2*C₆H₅CH₃

Base Information

• Chemical Name: Co₄O(O₂CC(CH₃)3)4(C₆H₅N₂C₇H₄C₄H₂NC₇H₄N₂C₆H₅)2*C₆H₅CH₃
• CAS No.: 503536-57-0
• Molecular Formula: C₇H₈*C₈₀H₇₆Co₄N₁₀O₉
• Molecular Weight: 1649.66
• Mol file: 503536-57-0.mol

Synonyms:

Chemical Property of Co₄O(O₂CC(CH₃)3)4(C₆H₅N₂C₇H₄C₄H₂NC₇H₄N₂C₆H₅)2*C₆H₅CH₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Co₄O(O₂CC(CH₃)3)4(C₆H₅N₂C₇H₄C₄H₂NC₇H₄N₂C₆H₅)2*C₆H₅CH₃

There total 1 articles about Co₄O(O₂CC(CH₃)3)4(C₆H₅N₂C₇H₄C₄H₂NC₇H₄N₂C₆H₅)2*C₆H₅CH₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

pyrrole-2,5-biscarboxaldehyde (39604-60-9) + N-phenyl-1,2-benzenediamine (534-85-0) → Co4O(O2CC(CH3)3)4(C6H5N2C7H4C4H2NC7H4N2C6H5)2*C6H5CH3 (503536-57-0)

Guidance literature:

With [Co(OH)n(OOCC(CH₃)3)(2-n)]x n=0.05-0.1; In acetonitrile; solid dicarbaldehyde and diamine (molar ratio 1:2) successively added tosoln. of Co polymer in MeCN; heated to 70°C for 10 min; concd.; toluene added; kept at 5°C for 2 d; decanted; crystals washed with cold MeCN; dried in vac. (25°C, 0.1 Torr); elem. anal.;

DOI:10.1023/A:1020995930577

upstream raw materials:

pyrrole-2,5-biscarboxaldehyde

N-phenyl-1,2-benzenediamine

Refernces