1,3-Dibenzylbenzene

Base Information

• Chemical Name: 1,3-Dibenzylbenzene
• CAS No.: 15180-20-8
• Molecular Formula: C20H18
• Molecular Weight: 258.363
• Mol file: 15180-20-8.mol

Synonyms:1,3-Dibenzyl-benzol;1,3-dibenzyl-benzene;m-dibenzylbenzene;

Chemical Property of 1,3-Dibenzylbenzene

Chemical Property:

• Boiling Point: 175 °C (1 mmHg)
• PSA: 0.00000
• LogP: 4.86820

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,3-Dibenzylbenzene

There total 46 articles about 1,3-Dibenzylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(ethoxymethyl)benzene (539-30-0) + benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → ethylbenzene (100-41-4,27536-89-6) + Diphenylmethane (101-81-5) + 1,4-dibenzylbenzene (793-23-7) + 1,3-dibenzylbenzene (15180-20-8)

Guidance literature:

Reference yield:

benzyl chloride (100-44-7) + benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → Diphenylmethane (101-81-5) + 1,2-dibenzylbenzene (792-68-7) + 1,4-dibenzylbenzene (793-23-7) + 1,3-dibenzylbenzene (15180-20-8)

Guidance literature:

With silica gel; for 0.25h; Product distribution; Ambient temperature;

DOI:10.1139/cjc-76-4-382

Reference yield:

benzyl alcohol (100-51-6,185532-71-2) + benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → Diphenylmethane (101-81-5) + 1,3-dibenzylbenzene (15180-20-8)

Guidance literature:

With toluene-4-sulfonic acid; Abdestillieren des entstehenden Wassers;

DOI:10.1021/ja01176a075

upstream raw materials:

1,3-dibenzoylbenzene

benzyl chloride

benzene

toluene-4-sulfonic acid

Downstream raw materials:

1,3-dibenzoylbenzene

Refernces

• 1、 Vinoth, Govindasamy,Indira, Sekar,Bharathi, Madheswaran,Nandhakumar, Arumugam,Sathishkumar, Kannappan,Shanmuga Bharathi, Kuppannan. "Synthesis, characterization, and catalytic activity of a new series of Ni(II), Cu(II), and Zn(II) complexes of N,N-O,O mixed-bidentate ligands for C–C cross-coupling reactions". . p. 3934 - 3946. Retrieved 2019/01/21.
• 2、 Li, Baiyan,Leng, Kunyue,Zhang, Yiming,Dynes, James J.,Wang, Jian,Hu, Yongfeng,Ma, Dingxuan,Shi, Zhan,Zhu, Liangkui,Zhang, Daliang,Sun, Yinyong,Chrzanowski, Matthew,Ma, Shengqian. "Metal-organic framework based upon the synergy of a Br?nsted acid framework and Lewis acid centers as a highly efficient heterogeneous catalyst for fixed-bed reactions". supporting information. p. 4243 - 4248. Retrieved 2015/04/14.