2,4,6-Tris(2-chloroethyl)-1,3,5-trioxane

Base Information

• Chemical Name: 2,4,6-Tris(2-chloroethyl)-1,3,5-trioxane
• CAS No.: 15678-07-6
• Molecular Formula: C9H15Cl3O3
• Molecular Weight: 277.5726
• Hs Code.: 2934999090
• Mol file: 15678-07-6.mol

Synonyms:2.4.6-Tris-<2-chlor-aethyl>-1.3.5-trioxan;

Chemical Property of 2,4,6-Tris(2-chloroethyl)-1,3,5-trioxane

Chemical Property:

• Vapor Pressure: 7.19E-05mmHg at 25°C
• Boiling Point: 353.7°Cat760mmHg
• Flash Point: 131.9°C
• PSA: 27.69000
• Density: 1.225g/cm³
• LogP: 2.91480

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,4,6-Tris(2-chloroethyl)-1,3,5-trioxane

There total 3 articles about 2,4,6-Tris(2-chloroethyl)-1,3,5-trioxane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

acrolein (107-02-8,25068-14-8) → 2,4,6-tris(2'-chloroethyl)-1,3,5-trioxane (15678-07-6) + 3-chloropropanaldehyde (19434-65-2)

Guidance literature:

With hydrogenchloride; In diethyl ether; at -42 ℃;

DOI:10.1039/P19830000717

Reference yield:

acrolein (107-02-8,25068-14-8) → 2,4,6-tris(2'-chloroethyl)-1,3,5-trioxane (15678-07-6)

Guidance literature:

With hydrogenchloride; sulfuric acid; sodium chloride; at 20 ℃; Cooling with ice;

DOI:10.1246/bcsj.20150387

Reference yield:

→ 2,4,6-tris(2'-chloroethyl)-1,3,5-trioxane (15678-07-6)

Guidance literature:

β-Chlor-propionaldehyd;

upstream raw materials:

acrolein

Refernces

• 1、 Hayashi, Daijiro,Narisawa, Tomoyuki,Masui, Yoichi,Onaka, Makoto. "H-type zeolite-catalyzed 1,4-addition of benzene derivatives to labile acrolein". supporting information. p. 460 - 471. Retrieved 2016/04/26.